Lectures

1-14  Introduction
Before Class:  Bring two copies of your favorite 3-5 page peer reviewed article to class.
We will review papers in class for format and content.
Activity:  Paper Format and Reading Assignment
Drake 1997- KENSHU method of paper reading comprehension
2016 Paper Format Discussion
Powerpoint- CHEM 314 Introduction
2016 Techniques

1-18 Introduction to Measurements
Reading:  Skoog ‘n’ Holler Chapter 1
Powerpoint- Intro to measurements

1-21 Noise & Error
Reading:  
Skoog ‘n’ Holler Chapter 5
Sources of error in the laboratory
Powerpoint-  Error and Noise

1-21  Planning Safe Experiments
Reading:  
How to Read and Understand a MSDS
Before Class:  
Bring one copy of MSDS sheets from 3 different vendors (including sigma aldrich) for one ingredient in your product.
Ansell  glove-chemical compatibility literature

1-25  Interactions of Light and Matter
Reading:  Skoog ‘n’ Holler Chapter 6
Powerpoint- Light and Matter Interactions

1-25 Project Overview Assignment
Endnote tutorial

1-26  Beer’s Law
Reading:  Skoog ‘n’ Holler Chapter  13
Beers Law Derivation
Powerpoint-  Beer’s law

2-1  Components of Optical Instruments
Reading:  
Skoog ‘n’ Holler Chapter  7
Powerpoint-  Components of Optical Instruments

2-2  Atomic Spectroscopy
Reading:  Skoog ‘n’ Holler Chapter 8-11
Powerpoint-Atomic Spectroscopy

2-8  Molecular  Spectroscopy
Reading:  
Skoog ‘n’ Holler Chapter  13-15
Powerpoint-  Molecular Spectoscopy

2-15  Vibrational Spectroscopy
Reading:  
Skoog ‘n’ Holler Chapter  16-18
FT-IR Newport Reading
Before  coming to class, respond to the following questions:
1. how does IR radiation interact with matter?
2. Why does FT-IR require an interferometer?
3. Describe how an interferometer works.  Draw an example  interferogram and label axes.
Resources:  IR and Raman Spectroscopy overview
Powerpoint-  FT-IR

2-22  Electron Microscopy
Reading:    SEM website,  EM video
Powerpoint-  electron microscopy

2-29    X-Ray  Techniques
Reading:    XRF  website,  XRD  or  XRD  website.
Synchrotron primer
Powerpoint-  x-ray techniques

2-29   Exam Review and Peer Review
Peer Review:  Peer Review Worksheet
Reading:  Nicholas et al., 2011- Peer review

3-7 Exam 1  
The exam will focus on assessing your understanding of material presented in class and lab.  The goal of the exam is for you to apply  knowledge to experimental situations.
Bring a nonprogrammable calculator.  Unusual formulas will be provided, but will expect that you know M1V1=M2V2, Beers Law, and other common formulas.
2014 CHEM 314 Exam 1    (key)
2015 CHEM 314 Exam 1  (key)
2016 CHEM 314 Exam 1 (key)
2015 Exam 1 equations

3-21   Chromatography
Reading:  
Skoog ‘n’ Holler Chapter  26
Before  coming to class, fill in pgs 1-2 in the class notes
chromatography class notes
Check out the info for the column we will be using in class:  Agilent Eclipse C18
Powerpoint-  Chromatography

3-28  Mass Spectrometry
Reading:  Skoog ‘n’ Holler Chapter 11, 20
Powerpoint-  Mass spec

4-4  Separations Instrumentation
Reading:  Skoog ‘n’ Holler Chapter  27-28
Powerpoint-  Separations

4-2 to 4-19 Throughput of an Optical Instrument
Reading:  
Skoog ‘n’ Holler Chapter  3, 7
Powerpoint-  Throughput

5-2 Exam Review
Come  with questions!
Final exam equations
2014 CHEM 314 Exam 2